Reconstructing the fractal clusters of detonation nanodiamonds from small-angle X-ray scattering

Research output: Contribution to journal › Journal article › Research › peer-review

Standard

Reconstructing the fractal clusters of detonation nanodiamonds from small-angle X-ray scattering. / Kowalczyk, Piotr; Piña-Salazar, Elda Zoraida; Kirkensgaard, Jacob Judas Kain; Terzyk, Artur P.; Futamura, Ryusuke; Hayashi, Takuya; Ōsawa, Eiji; Kaneko, Katsumi; Ciach, Alina.

In: Carbon, Vol. 169, 2020, p. 349-356.

Research output: Contribution to journal › Journal article › Research › peer-review

Harvard

Kowalczyk, P, Piña-Salazar, EZ, Kirkensgaard, JJK, Terzyk, AP, Futamura, R, Hayashi, T, Ōsawa, E, Kaneko, K & Ciach, A 2020, 'Reconstructing the fractal clusters of detonation nanodiamonds from small-angle X-ray scattering', Carbon, vol. 169, pp. 349-356. https://doi.org/10.1016/j.carbon.2020.08.003

APA

Kowalczyk, P., Piña-Salazar, E. Z., Kirkensgaard, J. J. K., Terzyk, A. P., Futamura, R., Hayashi, T., Ōsawa, E., Kaneko, K., & Ciach, A. (2020). Reconstructing the fractal clusters of detonation nanodiamonds from small-angle X-ray scattering. Carbon, 169, 349-356. https://doi.org/10.1016/j.carbon.2020.08.003

Vancouver

Kowalczyk P, Piña-Salazar EZ, Kirkensgaard JJK, Terzyk AP, Futamura R, Hayashi T et al. Reconstructing the fractal clusters of detonation nanodiamonds from small-angle X-ray scattering. Carbon. 2020;169:349-356. https://doi.org/10.1016/j.carbon.2020.08.003

Author

Kowalczyk, Piotr ; Piña-Salazar, Elda Zoraida ; Kirkensgaard, Jacob Judas Kain ; Terzyk, Artur P. ; Futamura, Ryusuke ; Hayashi, Takuya ; Ōsawa, Eiji ; Kaneko, Katsumi ; Ciach, Alina. / Reconstructing the fractal clusters of detonation nanodiamonds from small-angle X-ray scattering. In: Carbon. 2020 ; Vol. 169. pp. 349-356.

Bibtex

@article{be38f15a0b7e410788de1eb9aba58aed,
title = "Reconstructing the fractal clusters of detonation nanodiamonds from small-angle X-ray scattering",
abstract = "Detonation nanodiamonds (DND) form fractal-like aggregates composed of polydisperse DND particles. We present a novel methodology for the visualisation and characterisation of fractal clusters of DND from one-dimensional small-angle X-ray scattering (SAXS) intensity. The fractal nature and polydispersity of DND are modelled by combining a diffusion-limited aggregation (DLA) process implemented in Monte Carlo simulations with the distribution of DND sizes measured from high-resolution transmission electron microscopy. The radius of gyration (42–44 nm), aggregation number (850–1150), and the maximum dimension (226–242 nm) of DND fractal clusters were obtained from the fitting of the synchrotron-based SAXS data (q∼0.11–4.75 1/nm) measured for two samples of commercialized DND powders by the developed theoretical model.",
keywords = "Detonation nanodiamonds, Diffusion-limited aggregation, High-resolution transmission electron microscopy, Monte Carlo simulations, Radius of gyration, Small-angle X-ray scattering",
author = "Piotr Kowalczyk and Pi{\~n}a-Salazar, {Elda Zoraida} and Kirkensgaard, {Jacob Judas Kain} and Terzyk, {Artur P.} and Ryusuke Futamura and Takuya Hayashi and Eiji Ōsawa and Katsumi Kaneko and Alina Ciach",
year = "2020",
doi = "10.1016/j.carbon.2020.08.003",
language = "English",
volume = "169",
pages = "349--356",
journal = "Carbon",
issn = "0008-6223",
publisher = "Pergamon Press",

}

RIS

TY - JOUR

T1 - Reconstructing the fractal clusters of detonation nanodiamonds from small-angle X-ray scattering

AU - Kowalczyk, Piotr

AU - Piña-Salazar, Elda Zoraida

AU - Kirkensgaard, Jacob Judas Kain

AU - Terzyk, Artur P.

AU - Futamura, Ryusuke

AU - Hayashi, Takuya

AU - Ōsawa, Eiji

AU - Kaneko, Katsumi

AU - Ciach, Alina

PY - 2020

Y1 - 2020

N2 - Detonation nanodiamonds (DND) form fractal-like aggregates composed of polydisperse DND particles. We present a novel methodology for the visualisation and characterisation of fractal clusters of DND from one-dimensional small-angle X-ray scattering (SAXS) intensity. The fractal nature and polydispersity of DND are modelled by combining a diffusion-limited aggregation (DLA) process implemented in Monte Carlo simulations with the distribution of DND sizes measured from high-resolution transmission electron microscopy. The radius of gyration (42–44 nm), aggregation number (850–1150), and the maximum dimension (226–242 nm) of DND fractal clusters were obtained from the fitting of the synchrotron-based SAXS data (q∼0.11–4.75 1/nm) measured for two samples of commercialized DND powders by the developed theoretical model.

AB - Detonation nanodiamonds (DND) form fractal-like aggregates composed of polydisperse DND particles. We present a novel methodology for the visualisation and characterisation of fractal clusters of DND from one-dimensional small-angle X-ray scattering (SAXS) intensity. The fractal nature and polydispersity of DND are modelled by combining a diffusion-limited aggregation (DLA) process implemented in Monte Carlo simulations with the distribution of DND sizes measured from high-resolution transmission electron microscopy. The radius of gyration (42–44 nm), aggregation number (850–1150), and the maximum dimension (226–242 nm) of DND fractal clusters were obtained from the fitting of the synchrotron-based SAXS data (q∼0.11–4.75 1/nm) measured for two samples of commercialized DND powders by the developed theoretical model.

KW - Detonation nanodiamonds

KW - Diffusion-limited aggregation

KW - High-resolution transmission electron microscopy

KW - Monte Carlo simulations

KW - Radius of gyration

KW - Small-angle X-ray scattering

U2 - 10.1016/j.carbon.2020.08.003

DO - 10.1016/j.carbon.2020.08.003

M3 - Journal article

AN - SCOPUS:85089688486

VL - 169

SP - 349

EP - 356

JO - Carbon

JF - Carbon

SN - 0008-6223

ER -

ID: 248029809