1-(1-cyanocyclohexyl)-1-hydroxy-3-phenylurea

Research output: Contribution to journal › Journal article › Research › peer-review

Standard

1-(1-cyanocyclohexyl)-1-hydroxy-3-phenylurea. / Frydenvang, Karla; Larsen, Ingrid Kjøller.

In: Acta Crystallographica Section C: Crystal Structure Communications, Vol. 53, No. 8, 15.08.1997, p. 1091-1093.

Research output: Contribution to journal › Journal article › Research › peer-review

Harvard

Frydenvang, K & Larsen, IK 1997, '1-(1-cyanocyclohexyl)-1-hydroxy-3-phenylurea', Acta Crystallographica Section C: Crystal Structure Communications, vol. 53, no. 8, pp. 1091-1093. https://doi.org/10.1107/S0108270197004617

APA

Frydenvang, K., & Larsen, I. K. (1997). 1-(1-cyanocyclohexyl)-1-hydroxy-3-phenylurea. Acta Crystallographica Section C: Crystal Structure Communications, 53(8), 1091-1093. https://doi.org/10.1107/S0108270197004617

Vancouver

Frydenvang K, Larsen IK. 1-(1-cyanocyclohexyl)-1-hydroxy-3-phenylurea. Acta Crystallographica Section C: Crystal Structure Communications. 1997 Aug 15;53(8):1091-1093. https://doi.org/10.1107/S0108270197004617

Author

Frydenvang, Karla ; Larsen, Ingrid Kjøller. / 1-(1-cyanocyclohexyl)-1-hydroxy-3-phenylurea. In: Acta Crystallographica Section C: Crystal Structure Communications. 1997 ; Vol. 53, No. 8. pp. 1091-1093.

Bibtex

@article{ca5a149392b4484fb5adb5aea0afaef6,
title = "1-(1-cyanocyclohexyl)-1-hydroxy-3-phenylurea",
abstract = "In the crystals of the title compound, C14H17N3O2, there are two molecules (A and B) in the asymmetric unit. The conformation of the hydroxamic acid moiety, O=C-N-O, is antiperiplanar for both molecules. The phenyl substituent is in a synperiplanar conformation, with O=C-N-C torsion angles of 1.8 (2) and 2.1 (2)° for A and B, respectively. The corresponding torsion angles of the cyclohexyl substituents are -32.0 (2) and -30.8 (2)°, respectively. The cyclohexyl ring adopts a chair conformation in both molecules, with the hydroxamic acid moiety in an equatorial position and the cyano group in an axial position. The plane of the phenyl group is twisted with respect to the central urea plane [38.71 (7) and 43.08(7)° for molecules A and B, respectively]. No other significant differences in bond lengths, angles or torsion angles between molecules A and B are observed. The crystal packing shows that the A and B molecules are interconnected by hydrogen bonds, OH⋯O and NH⋯N, in the direction of the a axis.",
author = "Karla Frydenvang and Larsen, {Ingrid Kj{\o}ller}",
year = "1997",
month = aug,
day = "15",
doi = "10.1107/S0108270197004617",
language = "English",
volume = "53",
pages = "1091--1093",
journal = "Acta crystallographica. Section C, Structural chemistry",
issn = "2053-2296",
publisher = "Wiley",
number = "8",

}

RIS

TY - JOUR

T1 - 1-(1-cyanocyclohexyl)-1-hydroxy-3-phenylurea

AU - Frydenvang, Karla

AU - Larsen, Ingrid Kjøller

PY - 1997/8/15

Y1 - 1997/8/15

N2 - In the crystals of the title compound, C14H17N3O2, there are two molecules (A and B) in the asymmetric unit. The conformation of the hydroxamic acid moiety, O=C-N-O, is antiperiplanar for both molecules. The phenyl substituent is in a synperiplanar conformation, with O=C-N-C torsion angles of 1.8 (2) and 2.1 (2)° for A and B, respectively. The corresponding torsion angles of the cyclohexyl substituents are -32.0 (2) and -30.8 (2)°, respectively. The cyclohexyl ring adopts a chair conformation in both molecules, with the hydroxamic acid moiety in an equatorial position and the cyano group in an axial position. The plane of the phenyl group is twisted with respect to the central urea plane [38.71 (7) and 43.08(7)° for molecules A and B, respectively]. No other significant differences in bond lengths, angles or torsion angles between molecules A and B are observed. The crystal packing shows that the A and B molecules are interconnected by hydrogen bonds, OH⋯O and NH⋯N, in the direction of the a axis.

AB - In the crystals of the title compound, C14H17N3O2, there are two molecules (A and B) in the asymmetric unit. The conformation of the hydroxamic acid moiety, O=C-N-O, is antiperiplanar for both molecules. The phenyl substituent is in a synperiplanar conformation, with O=C-N-C torsion angles of 1.8 (2) and 2.1 (2)° for A and B, respectively. The corresponding torsion angles of the cyclohexyl substituents are -32.0 (2) and -30.8 (2)°, respectively. The cyclohexyl ring adopts a chair conformation in both molecules, with the hydroxamic acid moiety in an equatorial position and the cyano group in an axial position. The plane of the phenyl group is twisted with respect to the central urea plane [38.71 (7) and 43.08(7)° for molecules A and B, respectively]. No other significant differences in bond lengths, angles or torsion angles between molecules A and B are observed. The crystal packing shows that the A and B molecules are interconnected by hydrogen bonds, OH⋯O and NH⋯N, in the direction of the a axis.

UR - http://www.scopus.com/inward/record.url?scp=0031211555&partnerID=8YFLogxK

U2 - 10.1107/S0108270197004617

DO - 10.1107/S0108270197004617

M3 - Journal article

AN - SCOPUS:0031211555

VL - 53

SP - 1091

EP - 1093

JO - Acta crystallographica. Section C, Structural chemistry

JF - Acta crystallographica. Section C, Structural chemistry

SN - 2053-2296

IS - 8

ER -

ID: 382748211