Glycosylation intermediates studied using low temperature 1H- and 19F-DOSY NMR: new insight into the activation of trichloroacetimidates

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Low temperature 1H- and 19F-DOSY have been used for analyzing reactive intermediates in glycosylation reactions, where a glycosyl trichloroacetimidate donor has been activated using different catalysts. The DOSY protocols have been optimized for low temperature experiments and provided new insight into acid catalyzed glycosylation chemistry. From the study a new glycosylation intermediate was characterized.

Original languageEnglish
JournalChemical Communications
Volume52
Issue number76
Pages (from-to)11418-11421
Number of pages4
ISSN1359-7345
DOIs
Publication statusPublished - 2016

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